3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

Base Information

Chemical Name:3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate
CAS No.:1327280-81-8
Molecular Formula:C₁₆H₈F₇NO₃
Molecular Weight:395.233
Hs Code.:

Synonyms:3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

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Chemical Property of 3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

Chemical Property:

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Technology Process of 3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

There total 4 articles about 3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 434-64-0
perfluorotoluene

: 1327280-81-8
3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / 1,4-dioxane; water / 80 °C

2: toluene / 28 h / 20 °C / Reflux

With ammonium hydroxide; In 1,4-dioxane; water; toluene;
DOI:10.1002/anie.201102985

Reference yield:

: 651-83-2
4-trifluoromethyl-2,3,5,6-tetrafluoroaniline

: 16446-73-4
3-(chlorocarbonyl)phenyl acetate

: 1327280-81-8
3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

Guidance literature:: In toluene; at 20 ℃; for 28h; Reflux;
DOI:10.1002/anie.201102985

Reference yield:

: 6304-89-8
3-acetoxybenzoic acid

: 1327280-81-8
3-((2,3,5,6-tetrafluoro-4-(trifluoromethyl)phenyl)carbamoyl)phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: 0 - 20 °C / Inert atmosphere

2: toluene / 28 h / 20 °C / Reflux

In toluene;
DOI:10.1002/anie.201102985