4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

Base Information

Chemical Name:4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine
CAS No.:618863-12-0
Molecular Formula:C₂₀H₂₈N₆O₂
Molecular Weight:384.481
Hs Code.:

Synonyms:4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

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Chemical Property of 4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

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Technology Process of 4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

There total 2 articles about 4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 110-89-4
piperidine

: 618863-11-9
4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-2-methylthio-5-nitropyrimidine

: 618863-12-0
4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1016/j.tetlet.2003.09.112

Reference yield:

: 103-67-3
benzyl-methyl-amine

: 618863-12-0
4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: diisopropylethylamine / tetrahydrofuran / 0.33 h / 20 °C

1.2: 98 percent / tetrahydrofuran / 3 h / 20 °C

2.1: 88 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 18 h / 20 °C

With N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2003.09.112

Reference yield: 85.0%

: 1445-45-0
Trimethyl orthoacetate

: 618863-12-0
4-(N,N-Benzylmethylamino)-6-(N-isopropylamino)-5-nitro-2-piperidinylpyrimidine

: 9-Isopropyl-8-methyl-6-N,N-methylbenzylamino-2-piperidinylpurine

Guidance literature:: With chromium dichloride; methanesulfonic acid; In methanol; N,N-dimethyl-formamide; at 20 - 100 ℃; for 28h;
DOI:10.1016/j.tetlet.2003.09.112