pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

Base Information

Chemical Name:pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate
CAS No.:1101860-03-0
Molecular Formula:C₂₂H₂₀F₅NO₄
Molecular Weight:457.397
Hs Code.:

Synonyms:pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

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Technology Process of pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

There total 1 articles about pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1101859-92-0
N-tert-butoxycarbonyl-((E)-3-phenylprop-2-enyl)aminoacetic acid

: 771-61-9
2,3,4,5,6-pentafluorophenol

: 1101860-03-0
pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

Guidance literature:: With dmap; 1,2-dichloro-ethane; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1016/j.tet.2008.09.044

Reference yield: 88.0%

: 497-25-6
dimethylenecyclourethane

: 1101860-03-0
pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate

: 1101860-07-4
tert-butyl 2-oxo-2-(2-oxo-oxazolidin-3-yl)((E)-3-phenylprop-2-enylethyl)carbamate

Guidance literature:: dimethylenecyclourethane; With isopropylmagnesium chloride; In tetrahydrofuran; at -15 ℃; for 0.333333h;

pentafluorophenyl N-tert-butoxycarbonyl((E)-(3-phenylprop-2-enyl)amino)acetate; In tetrahydrofuran; at -15 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2008.09.044