(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

Base Information

Chemical Name:(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate
CAS No.:1311272-21-5
Molecular Formula:C₃₃H₄₄O₆
Molecular Weight:536.709
Hs Code.:

Synonyms:(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

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Technology Process of (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

There total 6 articles about (Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.2%

: 1311272-24-8
(Z)-2-(3,4-dimethoxybenzylidene)-5-hydroxybenzo[b]furan-3-one

: 112-67-4
n-hexadecanoyl chloride

: 1311272-21-5
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

Guidance literature:: With pyridine; In dichloromethane; Reflux;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-35-1
2'-hydroxy-5'-(methoxymethoxy)-3,4-dimethoxychalcone

: 1311272-21-5
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; mercury(II) diacetate / 1 h / 110 °C

2: hydrogenchloride; water / methanol / 0.5 h / Reflux

3: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; mercury(II) diacetate; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063

Reference yield:

: 1311272-28-2
(Z)-2-(3,4-dimethoxybenzylidene)-5-(methoxymethoxy)benzo[b]furan-3-one

: 1311272-21-5
(Z)-2-(3,4-dimethoxybenzylidene)-3-oxo-2,3-dihydrobenzofuran-5-yl palmitate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / methanol / 0.5 h / Reflux

2: pyridine / dichloromethane / Reflux

With pyridine; hydrogenchloride; water; In methanol; dichloromethane;
DOI:10.1016/j.bmc.2011.03.063