2,2-d₂-phenethyl bromide

Base Information

Chemical Name:2,2-d₂-phenethyl bromide
CAS No.:23088-37-1
Molecular Formula:C₈H₉Br
Molecular Weight:187.048
Hs Code.:

Synonyms:2,2-d₂-phenethyl bromide

Suppliers and Price of 2,2-d₂-phenethyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,2-d₂-phenethyl bromide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,2-d₂-phenethyl bromide

There total 13 articles about 2,2-d₂-phenethyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 51086-45-4
2,2-dideuterio-2-phenyl-ethanol

: 23088-37-1
2,2-d₂-phenethyl bromide

Guidance literature:: With bromine; triphenylphosphine; In dichloromethane; for 1h; Ambient temperature;
DOI:10.1021/ja00165a053

Reference yield: 60.0%

: 2,2-d₂-phenethyl alcohol methanesulfonate

: 23088-37-1
2,2-d₂-phenethyl bromide

Guidance literature:: With lithium bromide; In acetone; for 13h;
DOI:10.1021/ja000239f

Reference yield:

: 1076-07-9
2,2-dideuterio-2-phenyl-acetic acid

: 23088-37-1
2,2-d₂-phenethyl bromide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄ / tetrahydrofuran / 20 °C / overnight

2: Et₃N; 4-(dimethylamino)pyridine / CH₂Cl₂ / 16 h / 20 °C

3: 60 percent / LiBr / acetone / 13 h

With dmap; lithium aluminium tetrahydride; triethylamine; lithium bromide; In tetrahydrofuran; dichloromethane; acetone; 1: Reduction / 2: Addition / 3: Bromination;
DOI:10.1021/ja000239f