benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

Base Information

Chemical Name:benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside
CAS No.:104875-53-8
Molecular Formula:C₂₀H₂₀FN₃O₄
Molecular Weight:385.395
Hs Code.:

Synonyms:benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

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Chemical Property of benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

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Technology Process of benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

There total 3 articles about benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 104875-52-7
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-2-O-<(trifluoromethyl)sulfonyl>-β-D-idopyranoside

: 104875-53-8
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

Guidance literature:: With cesium fluoride; In N,N-dimethyl-formamide; at 70 ℃; for 5h;
DOI:10.1021/jo00374a013

Reference yield:

: 26531-94-2
benzyl 2,3-anhydro-4,6-O-benzylidene-β-D-talopyranoside

: 104875-53-8
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / sodium azide, ammonium chloride / 2-methoxy-ethanol; H₂O / 140 °C

2: 90 percent / pyridine / 5 h / Ambient temperature

3: 71 percent / cesium fluoride / dimethylformamide / 5 h / 70 °C

With pyridine; sodium azide; ammonium chloride; cesium fluoride; In 2-methoxy-ethanol; water; N,N-dimethyl-formamide;
DOI:10.1021/jo00374a013

Reference yield:

: 104875-51-6
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

: 104875-53-8
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 5 h / Ambient temperature

2: 71 percent / cesium fluoride / dimethylformamide / 5 h / 70 °C

With pyridine; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00374a013