benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

Base Information

Chemical Name:benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside
CAS No.:104875-51-6
Molecular Formula:C₂₀H₂₁N₃O₅
Molecular Weight:383.404
Hs Code.:

Synonyms:benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

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Technology Process of benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

There total 1 articles about benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 26531-94-2
benzyl 2,3-anhydro-4,6-O-benzylidene-β-D-talopyranoside

: 104875-51-6
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

Guidance literature:: With sodium azide; ammonium chloride; In 2-methoxy-ethanol; water; at 140 ℃;
DOI:10.1021/jo00374a013

Reference yield: 85.0%

: 104875-51-6
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

: 104875-54-9
3-azido-2-O-benzyl-4,6-O-benzylidene-3-deoxy-α-D-idopyranosyl fluoride

Guidance literature:: With diethylamino-sulfur trifluoride; In benzene; for 1h; Heating;
DOI:10.1021/jo00374a013

Reference yield:

: 104875-51-6
benzyl 3-azido-4,6-O-benzylidene-3-deoxy-β-D-idopyranoside

: 104875-53-8
benzyl 3-azido-4,6-O-benzylidene-2,3-dideoxy-2-fluoro-β-D-gulopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 5 h / Ambient temperature

2: 71 percent / cesium fluoride / dimethylformamide / 5 h / 70 °C

With pyridine; cesium fluoride; In N,N-dimethyl-formamide;
DOI:10.1021/jo00374a013