9-fluorenylmethyloxycarbonyl tyrosine leucine

Base Information

Chemical Name:9-fluorenylmethyloxycarbonyl tyrosine leucine
CAS No.:214612-70-1
Molecular Formula:C₃₀H₃₂N₂O₆
Molecular Weight:516.594
Hs Code.:

Synonyms:9-fluorenylmethyloxycarbonyl tyrosine leucine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-fluorenylmethyloxycarbonyl tyrosine leucine

Chemical Property:

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Technology Process of 9-fluorenylmethyloxycarbonyl tyrosine leucine

There total 5 articles about 9-fluorenylmethyloxycarbonyl tyrosine leucine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.7%

: 9-fluorenylmethyloxycarbonyl tyrosine leucine tert butyl ester

: 214612-70-1
9-fluorenylmethyloxycarbonyl tyrosine leucine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1039/c3cc45822a

Reference yield:

: 35661-60-0
Fmoc-Leu-OH

: 112883-29-1,92954-90-0
N-Fmoc-Tyr-OH

: 214612-70-1
9-fluorenylmethyloxycarbonyl tyrosine leucine

Guidance literature:: Fmoc-Leu-OH; With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; Inert atmosphere; solid phase reaction;

With dmap; In N,N-dimethyl-formamide; at 20 ℃; for 2h; solid phase reaction;

N-Fmoc-Tyr-OH; Further stages;
DOI:10.1039/b816847d

Reference yield:

: 220886-40-8
Fmoc-Tyr-Ala-OH

: 35661-60-0
Fmoc-Leu-OH

: 214612-70-1
9-fluorenylmethyloxycarbonyl tyrosine leucine

: 1122069-06-0
Fmoc-Tyr-Ala-Leu-OH

Guidance literature:: Fmoc-Leu-OH; With diisopropyl-carbodiimide; In dichloromethane; at 20 ℃; Inert atmosphere; solid phase reaction;

With dmap; In N,N-dimethyl-formamide; at 20 ℃; for 2h; solid phase reaction;

Fmoc-Tyr-Ala-OH; Further stages;
DOI:10.1039/b816847d