Technology Process of C15H20N2O2
There total 6 articles about C15H20N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
Noyori's catalyst; acetic acid; triethylamine;
In
ethanol; ethyl acetate;
at 20 ℃;
for 18h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 20 - 60 °C
1.2: 18 h / 60 °C
2.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / -35 °C
2.2: 1 h / 0 °C
3.1: Noyori's catalyst; acetic acid; triethylamine / ethanol; ethyl acetate / 18 h / 20 °C / Inert atmosphere
With
Noyori's catalyst; potassium tert-butylate; sodium hydride; acetic acid; triethylamine;
In
tetrahydrofuran; ethanol; ethyl acetate; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.25 h / -35 °C
1.2: 1 h / 0 °C
2.1: Noyori's catalyst; acetic acid; triethylamine / ethanol; ethyl acetate / 18 h / 20 °C / Inert atmosphere
With
Noyori's catalyst; potassium tert-butylate; acetic acid; triethylamine;
In
tetrahydrofuran; ethanol; ethyl acetate;