4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

Base Information

Chemical Name:4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside
CAS No.:176040-01-0
Molecular Formula:C₂₄H₃₁NO₆
Molecular Weight:429.513
Hs Code.:

Synonyms:4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

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Chemical Property of 4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

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Technology Process of 4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

There total 5 articles about 4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 176040-00-9
Acetic acid (2S,3S,4R,5R,6S)-3,5-dimethoxy-2-methyl-6-[4-(2-phenylacetylamino-ethyl)-phenoxy]-tetrahydro-pyran-4-yl ester

: 176040-01-0
4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: With potassium tert-butylate; In methanol; for 3h; Ambient temperature;
DOI:10.1016/0040-4020(96)00035-X

Reference yield:

: 51-67-2
tyrosamine

: 176040-01-0
4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 626 mg / aq. NaOH / ethanol / 39 h / Ambient temperature

2: 66 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / 0 °C

3: 89 percent / potassium tert-butoxide / methanol / 3 h / Ambient temperature

With sodium hydroxide; N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; potassium tert-butylate; In methanol; diethyl ether; ethanol; 1,2-dichloro-ethane;
DOI:10.1016/0040-4020(96)00035-X

Reference yield:

: 146399-58-8
ethyl 3-O-acetyl-2,4-di-O-methyl-1-thio-α-L-rhamnopyranoside

: 176040-01-0
4-<2-(benzylcarbonylamino)ethyl>phenyl 2,4-di-O-methyl-α-L-rhamnopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 66 percent / NIS, TfOH, molecular sieves 4 Angstroem / 1,2-dichloro-ethane; diethyl ether / 0.25 h / 0 °C

2: 89 percent / potassium tert-butoxide / methanol / 3 h / Ambient temperature

With N-iodo-succinimide; trifluorormethanesulfonic acid; 4 A molecular sieve; potassium tert-butylate; In methanol; diethyl ether; 1,2-dichloro-ethane;
DOI:10.1016/0040-4020(96)00035-X