C₃₃H₃₂Br₄N₄O₆

Base Information

Chemical Name:C₃₃H₃₂Br₄N₄O₆
CAS No.:884871-62-9
Molecular Formula:C₃₃H₃₂Br₄N₄O₆
Molecular Weight:900.256
Hs Code.:

C<sub>33</sub>H<sub>32</sub>Br<sub>4</sub>N<sub>4</sub>O<sub>6</sub>

Synonyms:C₃₃H₃₂Br₄N₄O₆

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Chemical Property of C₃₃H₃₂Br₄N₄O₆

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Technology Process of C₃₃H₃₂Br₄N₄O₆

There total 11 articles about C₃₃H₃₂Br₄N₄O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 884871-73-2
C₃₄H₃₆Br₄N₄O₇

: 884871-62-9
C₃₃H₃₂Br₄N₄O₆

Guidance literature:: With lead(IV) acetate; In benzene; at 20 ℃; for 0.166667h;
DOI:10.1021/jo060084f

Reference yield:

: 884871-43-6
C₁₇H₁₂ClN₃O₅

: 884871-62-9
C₃₃H₃₂Br₄N₄O₆

Guidance literature:: Multi-step reaction with 8 steps

1.1: 64 percent / DMAP; triethylamine / CH₂Cl₂ / 0.17 h / 20 °C

2.1: Zn; acetic acid / tetrahydrofuran / 20 °C

3.1: 91 percent / benzyltrimethylammonium tribromide; calcium carbonate / CH₂Cl₂; methanol / 0.5 h / 20 °C

4.1: 88 percent / CuBr₂; t-BuONO / acetonitrile / 1 h / 50 °C

5.1: 90 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1.5 h / 0 °C

6.1: LiHMDS / tetrahydrofuran / 0.58 h / -78 - 20 °C

6.2: 91 percent / tetrahydrofuran / 2 h / -78 °C

7.1: 99 percent / TFA / tetrahydrofuran; H₂O / 20 °C

8.1: Pb(OAc)4 / benzene / 0.17 h / 20 °C

With lead(IV) acetate; dmap; tert.-butylnitrite; ammonium cerium(IV) nitrate; benzyltrimethylammonium tribromide; acetic acid; triethylamine; trifluoroacetic acid; calcium carbonate; copper(ll) bromide; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jo060084f

Reference yield:

: 884871-44-7
C₂₂H₂₀ClN₃O₇

: 884871-62-9
C₃₃H₃₂Br₄N₄O₆

Guidance literature:: Multi-step reaction with 7 steps

1.1: Zn; acetic acid / tetrahydrofuran / 20 °C

2.1: 91 percent / benzyltrimethylammonium tribromide; calcium carbonate / CH₂Cl₂; methanol / 0.5 h / 20 °C

3.1: 88 percent / CuBr₂; t-BuONO / acetonitrile / 1 h / 50 °C

4.1: 90 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1.5 h / 0 °C

5.1: LiHMDS / tetrahydrofuran / 0.58 h / -78 - 20 °C

5.2: 91 percent / tetrahydrofuran / 2 h / -78 °C

6.1: 99 percent / TFA / tetrahydrofuran; H₂O / 20 °C

7.1: Pb(OAc)4 / benzene / 0.17 h / 20 °C

With lead(IV) acetate; tert.-butylnitrite; ammonium cerium(IV) nitrate; benzyltrimethylammonium tribromide; acetic acid; trifluoroacetic acid; calcium carbonate; copper(ll) bromide; lithium hexamethyldisilazane; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/jo060084f