2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

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Chemical Name:2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid
CAS No.:331628-17-2
Molecular Formula:C₁₆H₁₉N₃O₆S
Molecular Weight:381.409
Hs Code.:

Synonyms:2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

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Technology Process of 2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

There total 2 articles about 2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 117979-63-2
5-(p-chlorosulfonylbenzylidene)hydantoin

: 328-39-2,21675-61-6,25248-98-0,70-45-1
LEUCINE

: 331628-17-2
2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

Guidance literature:: With triethylamine; In tetrahydrofuran; water; at 20 ℃; for 2h;
DOI:10.1023/A:1017592817982

Reference yield:

: 3775-01-7
5-benzylidenehydantoin

: 331628-17-2
2-{4-[2,5-Dioxo-imidazolidin-(4Z)-ylidenemethyl]-benzenesulfonylamino}-4-methyl-pentanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / chlorosulfonic acid / 6 h / 20 °C

2: 72 percent / triethylamine / tetrahydrofuran; H₂O / 2 h / 20 °C

With chlorosulfonic acid; triethylamine; In tetrahydrofuran; water;
DOI:10.1023/A:1017592817982