1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

Base Information

Chemical Name:1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose
CAS No.:349654-64-4
Molecular Formula:C₂₂H₂₃BrF₂O₅
Molecular Weight:485.322
Hs Code.:

Synonyms:1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

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Chemical Property of 1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

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Technology Process of 1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

There total 3 articles about 1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 349654-64-4
1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOH; K₂CO₃ / dimethylsulfoxide

2: 310 mg / Et₃N; DMAP / CH₂Cl₂

With dmap; sodium hydroxide; potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1055/s-2001-13419

Reference yield:

: 153975-93-0
1,4-anhydro-2-deoxy-3,5-bis-O-(trimethylsilyl)-D-erythro-pent-1-enitol

: 349654-64-4
1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / NaOH; K₂CO₃ / dimethylsulfoxide

2: 310 mg / Et₃N; DMAP / CH₂Cl₂

With dmap; sodium hydroxide; potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1055/s-2001-13419

Reference yield:

: 50-89-5,28854-96-8,3545-96-8,50-88-4
thymidine

: 349654-64-4
1'-O-Acetyl-2'-deoxy-2'-bromodifluoromethyl-3',5'-di-O-benzyl-α-D-arabinose

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / (NH₄)2SO₄ / 9 h / Heating

2: 80 percent / NaOH; K₂CO₃ / dimethylsulfoxide

3: 310 mg / Et₃N; DMAP / CH₂Cl₂

With dmap; ammonium sulfate; sodium hydroxide; potassium carbonate; triethylamine; In dichloromethane; dimethyl sulfoxide;
DOI:10.1055/s-2001-13419