methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

Base Information

Chemical Name:methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate
CAS No.:126822-58-0
Molecular Formula:C₁₇H₁₈O₄S
Molecular Weight:318.394
Hs Code.:

Synonyms:methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

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Chemical Property of methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

Chemical Property:

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Technology Process of methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

There total 4 articles about methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 13291-18-4
isopropenylmagnesium bromide

: 126822-67-1
methyl 2-<(phenylthio)methyl>-5-formyl-3-furoate

: 126822-58-0
methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

Guidance literature:: In diethyl ether; at -30 ℃; for 0.5h;

Reference yield:

: 71483-05-1
methyl 3-oxo-4-(phenylthio)butanoate

: 126822-58-0
methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

Guidance literature:: Multi-step reaction with 4 steps

1: 18 h / Ambient temperature

2: glacial acetic acid, water / ethanol / 6 h / 80 °C / Heating

3: 1.) oxalyl chloride, dimethyl sulfoxide, 2.) triethylamine / 1.) dichloromethane, -60 deg C, 15 min, 2.) from -60 deg C to RT, 45 min

4: 74 percent / diethyl ether / 0.5 h / -30 °C

With oxalyl dichloride; water; acetic acid; dimethyl sulfoxide; triethylamine; In diethyl ether; ethanol;

Reference yield:

: 126822-57-9
methyl 2-<(phenylthio)methyl>-5-(hydroxymethyl)-3-furoate

: 126822-58-0
methyl 2-<(phenylthio)methyl>-5-(1-hydroxy-2-methyl-2-propenyl)-3-furoate

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) oxalyl chloride, dimethyl sulfoxide, 2.) triethylamine / 1.) dichloromethane, -60 deg C, 15 min, 2.) from -60 deg C to RT, 45 min

2: 74 percent / diethyl ether / 0.5 h / -30 °C

With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In diethyl ether;