C₃₈H₅₂O₄Si₂

Base Information

• Chemical Name: C₃₈H₅₂O₄Si₂
• CAS No.: 1521267-19-5
• Molecular Formula: C₃₈H₅₂O₄Si₂
• Molecular Weight: 628.999
• Mol file: 1521267-19-5.mol

Synonyms:C₃₈H₅₂O₄Si₂

Chemical Property of C₃₈H₅₂O₄Si₂

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₃₈H₅₂O₄Si₂

There total 6 articles about C₃₈H₅₂O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

C34H52O4Si2 (1521266-91-0) + benzaldehyde (100-52-7) → C38H52O4Si2 (1521267-19-5) + C38H52O4Si2

Guidance literature:

With trifluoroacetic acid; In chloroform; at 20 ℃; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/jacs.6b05127

Reference yield:

C34H52O4Si2 (1521266-91-0) + benzaldehyde (100-52-7) → C38H52O4Si2 + C38H52O4Si2 (1521267-19-5)

Guidance literature:

With trifluoroacetic acid; In chloroform; at 20 ℃; Overall yield = 93 %; Overall yield = 5.72 g; chemoselective reaction; Inert atmosphere;

DOI:10.1021/ja411270d

Reference yield:

tert-butylchlorodiphenylsilane (58479-61-1) → C38H52O4Si2 (1521267-19-5)

Guidance literature:

Multi-step reaction with 2 steps

1: dmap; pyridine / 12 h / 20 °C / Inert atmosphere

2: trifluoroacetic acid / chloroform / 20 °C / Inert atmosphere

With pyridine; dmap; trifluoroacetic acid; In chloroform;

DOI:10.1021/ja411270d

upstream raw materials:

tert-butylchlorodiphenylsilane

C₃₄H₅₂O₄Si₂

benzaldehyde

C₁₈H₃₄O₄Si

Downstream raw materials:

C₃₈H₅₀O₄Si₂

C₁₆H₁₈O₄

C₂₂H₂₈O₅

C₁₈H₂₀O₄