amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

Base Information

Chemical Name:amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester
CAS No.:1448674-61-0
Molecular Formula:C₁₈H₂₁N₃O₃
Molecular Weight:327.383
Hs Code.:

Synonyms:amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

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Chemical Property of amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

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Technology Process of amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

There total 4 articles about amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 1448674-60-9
5-benzyloxypyridine-2-carboxamidine

: 1448674-61-0
amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

Guidance literature:: 5-benzyloxypyridine-2-carboxamidine; With sodium hydrogencarbonate; In 1,4-dioxane; water; at 20 ℃; for 0.333333h;

di-tert-butyl dicarbonate; In 1,4-dioxane; water; at 20 ℃; for 16h;

Reference yield:

: 5-hydroxypyridine-2-carbonitrile

: 1448674-61-0
amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 60 °C

1.2: 1 h / 66 °C

2.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane / tetrahydrofuran; hexane / 16 h / 0 - 20 °C

3.1: sodium hydrogencarbonate / 1,4-dioxane; water / 0.33 h / 20 °C

3.2: 16 h / 20 °C

With n-butyllithium; sodium hydrogencarbonate; potassium carbonate; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; 1,4-dioxane; hexane; water; N,N-dimethyl-formamide;

Reference yield:

: 100-39-0
benzyl bromide

: 1448674-61-0
amino-(5-benzyloxypyridin-2-yl)methylene-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.5 h / 60 °C

1.2: 1 h / 66 °C

2.1: n-butyllithium; 1,1,1,3,3,3-hexamethyl-disilazane / tetrahydrofuran; hexane / 16 h / 0 - 20 °C

3.1: sodium hydrogencarbonate / 1,4-dioxane; water / 0.33 h / 20 °C

3.2: 16 h / 20 °C

With n-butyllithium; sodium hydrogencarbonate; potassium carbonate; 1,1,1,3,3,3-hexamethyl-disilazane; In tetrahydrofuran; 1,4-dioxane; hexane; water; N,N-dimethyl-formamide;