(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

Base Information

Chemical Name:(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine
CAS No.:183794-24-3
Molecular Formula:C₂₆H₃₉NO₃Si
Molecular Weight:441.686
Hs Code.:

Synonyms:(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

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Chemical Property of (S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

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Technology Process of (S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

There total 5 articles about (S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 85803-44-7
(S)-2-amino-3-(4-benzyloxyphenyl)-1-propanol

: 183794-23-2
(2Z)-4-[(tert-butyldimethylsilyl)oxy]but-2-en-1-yl methane-sulfonate

: 183794-24-3
(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

Guidance literature:: With potassium hydride; In diethyl ether; for 3h; Ambient temperature;
DOI:10.1021/jo961114p

Reference yield:

: 16652-64-5
O-benzyl-S-tyrosine

: 183794-24-3
(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / thionyl chloride / 72 h / Ambient temperature

2: 1.) triethylamine, 2.) LiAlH₄ / 1.) EtOAc, 1 h, 2.) THF, 2 h

3: 55 percent / KH / diethyl ether / 3 h / Ambient temperature

With lithium aluminium tetrahydride; thionyl chloride; potassium hydride; triethylamine; In diethyl ether;
DOI:10.1021/jo961114p

Reference yield:

: 91202-69-6,134297-05-5,113123-37-8
(Z)-4-(tert-butyldimethylsilyloxy)but-2-en-1-ol

: 183794-24-3
(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / triethylamine / CH₂Cl₂ / 3.5 h / Ambient temperature

2: 55 percent / KH / diethyl ether / 3 h / Ambient temperature

With potassium hydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1021/jo961114p