(S)-2-AMINO-3-[4-(PHENYLMETHOXY)PHENYL]-1-PROPANOL

Base Information

• Chemical Name: (S)-2-AMINO-3-[4-(PHENYLMETHOXY)PHENYL]-1-PROPANOL
• CAS No.: 85803-44-7
• Molecular Formula: C₁₆H₁₉NO₂
• Molecular Weight: 257.332
• Mol file: 85803-44-7.mol

Synonyms:(S)-2-amino-3-(4-benzyloxyphenyl)-1-propanol

Chemical Property of (S)-2-AMINO-3-[4-(PHENYLMETHOXY)PHENYL]-1-PROPANOL

Chemical Property:

• Storage Temp.: Store at 0-5°C

Purity/Quality:

98%min ^*data from raw suppliers

(S)-2-Amino-3-[4-(phenylmethoxy)phenyl]-1-propanol ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (S)-2-AMINO-3-[4-(PHENYLMETHOXY)PHENYL]-1-PROPANOL

There total 19 articles about (S)-2-AMINO-3-[4-(PHENYLMETHOXY)PHENYL]-1-PROPANOL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

O-benzyl N-Boc-L-tyrosinol (66605-58-1) → (S)-2-amino-3-(4-benzyloxyphenyl)-1-propanol (85803-44-7)

Guidance literature:

With toluene-4-sulfonic acid; In tetrahydrofuran; dichloromethane; for 6h; pH=13; Heating;

DOI:10.1021/ja074392m

Reference yield: 77.0%

O-benzyl-S-tyrosine (16652-64-5) → (S)-2-amino-3-(4-benzyloxyphenyl)-1-propanol (85803-44-7)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 6h;

DOI:10.1016/j.tetlet.2009.01.127

Reference yield:

morpholine (110-91-8,99108-56-2) + O-benzyl-N-tert-butoxycarbonyl-L-tyrosine (2130-96-3,54784-43-9) + chloroformic acid ethyl ester (541-41-3) → (S)-2-amino-3-(4-benzyloxyphenyl)-1-propanol (85803-44-7)

Guidance literature:

With 4-methyl-morpholine; hydrogenchloride; sodium tetrahydroborate; In tetrahydrofuran; methanol;

upstream raw materials:

O-benzyl-S-tyrosine

methyl 2S-amino-3-(4-benzyloxyphenyl)propionate hydrochloride

O-benzyl N-Boc-L-tyrosinol

L-Tyr-OMe

Downstream raw materials:

(4S)-4-(4'-benzyloxy)benzyl-4,5-dihydrooxazoline

(S)-1-(4-Benzyloxy-benzyl)-2-[(Z)-4-(tert-butyl-dimethyl-silanyloxy)-but-2-enyloxy]-ethylamine

(S)-4-(4-(benzyloxy)benzyl)oxazolidin-2-one

N₁,N₃-di{(1S)-1-[4-(benzyloxy)benzyl]-2-hydroxyethyl}-2,2-diethylmanonamide

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