(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

Base Information

Chemical Name:(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide
CAS No.:1026074-52-1
Molecular Formula:C₃₈H₅₈N₂O₁₅
Molecular Weight:782.883
Hs Code.:

(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

Synonyms:(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

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Chemical Property of (1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

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Technology Process of (1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

There total 2 articles about (1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1026074-51-0
C₅₁H₆₂O₁₈

: 107-15-3,85404-18-8
ethylenediamine

: 1026074-52-1
(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

Guidance literature:: at 70 ℃; for 7h;

Reference yield:

: 1026074-51-0
C₅₁H₆₂O₁₈

: 1026074-52-1
(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium methylate; methanol / 1 h / 20 °C

2: 3 h / 70 °C

With methanol; sodium methylate;

Reference yield: 48.0%

: 37149-18-1
1-oxyl-4-carboxyl-2,2,6,6-tetramethylpiperidine

: 1026074-52-1
(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide

: 1443747-71-4
C₄₈H₇₄N₃O₁₇

Guidance literature:: 1-oxyl-4-carboxyl-2,2,6,6-tetramethylpiperidine; With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; for 0.166667h;

(1R,3R,4R,5S)-N-(2-aminoethyl)-3-[2-O-benzoyl-3-O-((1S)-1-carboxy-2-cyclohexylethyl)-(β-D-galactopyranosyl)oxy]-4-[(α-L-fucopyranosyl)oxy]-5-methylcyclohexanecarboxamide; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 1h;
DOI:10.1021/ja4029582