C₃₀H₄₇ClO₃Si₂

Base Information

Chemical Name:C₃₀H₄₇ClO₃Si₂
CAS No.:913355-76-7
Molecular Formula:C₃₀H₄₇ClO₃Si₂
Molecular Weight:547.325
Hs Code.:

C<sub>30</sub>H<sub>47</sub>ClO<sub>3</sub>Si<sub>2</sub>

Synonyms:C₃₀H₄₇ClO₃Si₂

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Chemical Property of C₃₀H₄₇ClO₃Si₂

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Technology Process of C₃₀H₄₇ClO₃Si₂

There total 7 articles about C₃₀H₄₇ClO₃Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 865872-30-6
tert-butyl-((3R,4R)-4-chloro-3-methoxyhex-5-enyloxy)dimethylsilane

: 913355-76-7
C₃₀H₄₇ClO₃Si₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: K₃[Fe(CN)6]; hydroquinine 2,5-diphenyl-4,6-pyrimidinediyl diether; OsO₄ / 2-methyl-propan-2-ol; H₂O

2.1: pyridine

3.1: potassium carbonate / methanol

4.1: nBuLi / tetrahydrofuran / 0 °C

4.2: tetrahydrofuran / 0 °C

5.1: imidazole

With pyridine; 1H-imidazole; osmium(VIII) oxide; n-butyllithium; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1002/anie.200601655

Reference yield:

: 865872-31-7
(2R,3R,4R)-6-(tert-butyldimethylsilanyloxy)-3-chloro-4-methoxyhexane-1,2-diol

: 913355-76-7
C₃₀H₄₇ClO₃Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine

2.1: potassium carbonate / methanol

3.1: nBuLi / tetrahydrofuran / 0 °C

3.2: tetrahydrofuran / 0 °C

4.1: imidazole

With pyridine; 1H-imidazole; n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol;
DOI:10.1002/anie.200601655

Reference yield:

: 865872-29-3
(3R,4R)-1-(tert-butyldimethylsilanyloxy)-4-chlorohex-5-en-3-ol

: 913355-76-7
C₃₀H₄₇ClO₃Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: proton sponge

2.1: K₃[Fe(CN)6]; hydroquinine 2,5-diphenyl-4,6-pyrimidinediyl diether; OsO₄ / 2-methyl-propan-2-ol; H₂O

3.1: pyridine

4.1: potassium carbonate / methanol

5.1: nBuLi / tetrahydrofuran / 0 °C

5.2: tetrahydrofuran / 0 °C

6.1: imidazole

With pyridine; 1H-imidazole; osmium(VIII) oxide; n-butyllithium; Proton Sponge; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); potassium carbonate; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; water; tert-butyl alcohol;
DOI:10.1002/anie.200601655