Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Base Information

Chemical Name:Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester
CAS No.:177536-82-2
Molecular Formula:C₂₁H₂₆Cl₃NO₆S
Molecular Weight:526.866
Hs Code.:

Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Synonyms:Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

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Chemical Property of Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

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Technology Process of Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

There total 3 articles about Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 177536-81-1
Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

: 177536-82-2
Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Guidance literature:: With sodium methylate; In methanol; for 1h; Ambient temperature;

Reference yield:

: 108-98-5
thiophenol

: 177536-82-2
Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BF₃*Et₂O, Et₃N / CH₂Cl₂; diethyl ether / 48 h / Ambient temperature

2: 91 percent / MeONa / methanol / 1 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium methylate; triethylamine; In methanol; diethyl ether; dichloromethane;

Reference yield:

: 177536-80-0
6-O-Acetyl-2-O-(cyclohexylcarbamoyl)-3,4-O-(2,2,2-trichloroethylidene)-α-D-altropyranosyl fluoride

: 177536-82-2
Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / BF₃*Et₂O, Et₃N / CH₂Cl₂; diethyl ether / 48 h / Ambient temperature

2: 91 percent / MeONa / methanol / 1 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium methylate; triethylamine; In methanol; diethyl ether; dichloromethane;