Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

Base Information

Chemical Name:Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester
CAS No.:177536-81-1
Molecular Formula:C₂₃H₂₈Cl₃NO₇S
Molecular Weight:568.903
Hs Code.:

Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

Synonyms:Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

There total 1 articles about Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 108-98-5
thiophenol

: 177536-80-0
6-O-Acetyl-2-O-(cyclohexylcarbamoyl)-3,4-O-(2,2,2-trichloroethylidene)-α-D-altropyranosyl fluoride

: 177536-81-1
Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

Guidance literature:: With boron trifluoride diethyl etherate; triethylamine; In diethyl ether; dichloromethane; for 48h; Ambient temperature;

Reference yield: 91.0%

: 177536-81-1
Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

: 177536-82-2
Cyclohexyl-carbamic acid (2S,3aR,4R,6R,7S,7aR)-4-hydroxymethyl-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-7-yl ester

Guidance literature:: With sodium methylate; In methanol; for 1h; Ambient temperature;

Reference yield:

: 177536-81-1
Acetic acid (2S,3aR,4R,6R,7S,7aR)-7-cyclohexylcarbamoyloxy-6-phenylsulfanyl-2-trichloromethyl-tetrahydro-[1,3]dioxolo[4,5-c]pyran-4-ylmethyl ester

: C₃₈H₄₈Cl₆N₂O₁₃S

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / MeONa / methanol / 1 h / Ambient temperature

2: 93 percent / BF₃*Et₂O, Et₃N / CH₂Cl₂; diethyl ether / 4.5 h / Ambient temperature

With boron trifluoride diethyl etherate; sodium methylate; triethylamine; In methanol; diethyl ether; dichloromethane;