C₅₀H₇₇ClO₁₃Si

Base Information

Chemical Name:C₅₀H₇₇ClO₁₃Si
CAS No.:1392122-65-4
Molecular Formula:C₅₀H₇₇ClO₁₃Si
Molecular Weight:949.692
Hs Code.:

C<sub>50</sub>H<sub>77</sub>ClO<sub>13</sub>Si

Synonyms:C₅₀H₇₇ClO₁₃Si

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Chemical Property of C₅₀H₇₇ClO₁₃Si

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Technology Process of C₅₀H₇₇ClO₁₃Si

There total 5 articles about C₅₀H₇₇ClO₁₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 1392122-63-2
C₄₉H₇₉ClO₁₂Si

: 1392122-65-4
C₅₀H₇₇ClO₁₃Si

Guidance literature:: With pyridine; bis(trichloromethyl) carbonate; triethylamine; In dichloromethane; at -78 - 20 ℃; for 0.5h; Inert atmosphere;
DOI:10.1039/c2ob25101a

Reference yield:

: 916323-63-2
C₃₀H₄₉ClO₇Si

: 1392122-65-4
C₅₀H₇₇ClO₁₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate; Dess-Martin periodane / dichloromethane / 2 h / Inert atmosphere

2.1: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere

3.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / Inert atmosphere

3.2: 0.5 h

4.1: dimethyl sulfide borane / tetrahydrofuran / 4 h / Inert atmosphere

5.1: pyridine; bis(trichloromethyl) carbonate; triethylamine / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

With pyridine; bis(trichloromethyl) carbonate; dimethyl sulfide borane; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; 1.1: Dess-Martin oxidation / 2.1: Wittig olefination;
DOI:10.1039/c2ob25101a

Reference yield:

: 1032989-78-8
C₃₀H₄₇ClO₇Si

: 1392122-65-4
C₅₀H₇₇ClO₁₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 0.5 h / -78 - 20 °C / Inert atmosphere

2.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / Inert atmosphere

2.2: 0.5 h

3.1: dimethyl sulfide borane / tetrahydrofuran / 4 h / Inert atmosphere

4.1: pyridine; bis(trichloromethyl) carbonate; triethylamine / dichloromethane / 0.5 h / -78 - 20 °C / Inert atmosphere

With pyridine; bis(trichloromethyl) carbonate; dimethyl sulfide borane; triethylamine; 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; dichloromethane; 1.1: Wittig olefination;
DOI:10.1039/c2ob25101a