diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

Base Information

Chemical Name:diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate
CAS No.:141607-24-1
Molecular Formula:C₂₆H₃₀NO₁₂P
Molecular Weight:579.497
Hs Code.:

Synonyms:diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

Suppliers and Price of diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

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Technology Process of diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

There total 2 articles about diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 10294-12-9,10353-11-4,70749-28-9,76612-22-1,116559-73-0,147129-68-8,34051-43-9
2-deoxy-2-acetamido-3,4,6-tri-O-acetyl-D-glucopyranose

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 141607-24-1
diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

Guidance literature:: With dmap; In dichloromethane; at -30 - -25 ℃; for 2h;
DOI:10.1016/0008-6215(92)80015-S

Reference yield:

: 3068-34-6
Acetic acid (2R,3S,4R,5R,6R)-3-acetoxy-2-acetoxymethyl-5-acetylamino-6-chloro-tetrahydro-pyran-4-yl ester

: 141607-24-1
diphenyl (2-acetamido-3,4,6,-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl) phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Ag₂CO₃, H₂O / acetonitrile / 16 h / Ambient temperature

2: 62 percent / DMAP / CH₂Cl₂ / 2 h / -30 - -25 °C

With dmap; water; silver carbonate; In dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(92)80015-S