4-(3-pyridyl)butyl phenylpropynoate

Base Information

Chemical Name:4-(3-pyridyl)butyl phenylpropynoate
CAS No.:97607-58-4
Molecular Formula:C₁₈H₁₇NO₂
Molecular Weight:279.338
Hs Code.:

Synonyms:4-(3-pyridyl)butyl phenylpropynoate

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Chemical Property of 4-(3-pyridyl)butyl phenylpropynoate

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Technology Process of 4-(3-pyridyl)butyl phenylpropynoate

There total 3 articles about 4-(3-pyridyl)butyl phenylpropynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 60753-14-2
3-(4-hydroxybutyl)-pyridine

: 637-44-5
phenylpropyolic acid

: 97607-58-4
4-(3-pyridyl)butyl phenylpropynoate

Guidance literature:: With dicyclohexyl-carbodiimide; In tetrahydrofuran; 1.) -10 deg C, 2 h, 2.) RT, overnight;

Reference yield:

: 500-22-1
3-pyridinecarboxaldehyde

: 97607-58-4
4-(3-pyridyl)butyl phenylpropynoate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) n-butyl-lithium / 1.) THF/hexane, RT, 30 min, 2.) THF/hexane, -10 deg C, 1 h

2: 64 percent / H₂ / PtO / ethanol / 70 h

3: 88 percent / DCC / tetrahydrofuran / 1.) -10 deg C, 2 h, 2.) RT, overnight

With n-butyllithium; hydrogen; dicyclohexyl-carbodiimide; platinum(II) oxide; In tetrahydrofuran; ethanol;

Reference yield:

: 535972-85-1
4-(3-pyridyl)but-3-en-1-ol

: 97607-58-4
4-(3-pyridyl)butyl phenylpropynoate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / H₂ / PtO / ethanol / 70 h

2: 88 percent / DCC / tetrahydrofuran / 1.) -10 deg C, 2 h, 2.) RT, overnight

With hydrogen; dicyclohexyl-carbodiimide; platinum(II) oxide; In tetrahydrofuran; ethanol;