N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

Base Information

Chemical Name:N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride
CAS No.:1569982-75-7
Molecular Formula:C₂₆H₂₆N₄O₂*ClH
Molecular Weight:462.979
Hs Code.:

Synonyms:N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

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Chemical Property of N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

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Technology Process of N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

There total 9 articles about N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1569982-66-6
2-methoxy-5-(6-(2-methoxyphenyl)pyrimidin-4-ylamino)benzaldehyde

: 100-46-9
benzylamine

: 1569982-75-7
N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

Guidance literature:: 2-methoxy-5-(6-(2-methoxyphenyl)pyrimidin-4-ylamino)benzaldehyde; benzylamine; With ethanol; toluene-4-sulfonic acid; Reflux;

With sodium tetrahydroborate; at 20 ℃; for 3h;

With hydrogenchloride; In ethyl acetate;

Reference yield:

: 1569986-04-4
(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

: 1569982-75-7
N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C

2.1: manganese(IV) oxide / toluene / Reflux

3.1: toluene-4-sulfonic acid; ethanol / Reflux

3.2: 3 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; ethanol; toluene-4-sulfonic acid; In tetrahydrofuran; toluene;

Reference yield:

: 1569982-45-1
(2-methoxy-5-(6-(2-methoxyphenyl)pyrimidin-4-ylamino)phenyl)methanol

: 1569982-75-7
N-(3-((benzylamino)methyl)-4-methoxyphenyl)-6-(2-methoxyphenyl)pyrimidin-4-amine hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: manganese(IV) oxide / toluene / Reflux

2.1: toluene-4-sulfonic acid; ethanol / Reflux

2.2: 3 h / 20 °C

With manganese(IV) oxide; ethanol; toluene-4-sulfonic acid; In toluene;