(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

Base Information

Chemical Name:(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride
CAS No.:1569986-04-4
Molecular Formula:C₂₀H₁₉N₃O₄*ClH
Molecular Weight:401.849
Hs Code.:

Synonyms:(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

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Chemical Property of (4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

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Technology Process of (4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

There total 5 articles about (4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 99450-55-2
4-methoxy-3-methoxycarbonyl-phenyl-ammonium chloride

: 75634-03-6
4-chloro-6-(2-methoxy-phenyl)-pyrimidine

: 1569986-04-4
(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

Guidance literature:: In tert-butyl alcohol; for 6h; Reflux;

Reference yield:

: 5720-06-9
2-Methoxyphenylboronic acid

: 1569986-04-4
(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

Guidance literature:: Multi-step reaction with 2 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / water; 1,2-dimethoxyethane / 2 h / Inert atmosphere; Reflux

2: tert-butyl alcohol / 6 h / Reflux

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,2-dimethoxyethane; water; tert-butyl alcohol;

Reference yield:

: 2-methoxy-5-nitro-benzoic acid sodium salt

: 1569986-04-4
(4-methoxy-3-methoxycarbonyl-phenyl)-[6-(2-methoxy-phenyl)-pyrimidin-4-yl]-ammonium chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 0 °C

1.2: Reflux

2.1: tin(II) chloride dihdyrate / methanol / 24 h / Reflux

2.2: 0.5 h / 0 °C

3.1: tert-butyl alcohol / 6 h / Reflux

With thionyl chloride; tin(II) chloride dihdyrate; In methanol; tert-butyl alcohol;