2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate

Base Information

• Chemical Name: 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate
• CAS No.: 73669-89-3
• Molecular Formula: C₂F₃O₂*C₂₂H₂₁OS
• Molecular Weight: 446.49

Synonyms:2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate

Chemical Property of 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate

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Technology Process of 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate

There total 5 articles about 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

1-(p-Methoxyphenyl)-3-phenyl-3-(2'-oxocyclohexyl)-1-propanone (73669-78-0) → 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate (73669-89-3)

Guidance literature:

With hydrogen sulfide; In trifluoroacetic acid; 1.) 3 h, 2.) heating on water bath.;

DOI:10.1007/BF00476376

Reference yield: 28.0%

1-(p-Methoxyphenyl)-3-phenyl-3-(2'-oxocyclohexyl)-1-propanone (73669-78-0) → 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate (73669-89-3) + 3-(4-Methoxyphenyl)-5-phenyl-2-thiabicyclo<4.4.0>decane (73669-96-2)

Guidance literature:

With hydrogen sulfide; In trifluoroacetic acid; Yields of byproduct given; 1.) room temperature, overnight; 2.) reflux;

Reference yield: 28.0%

1-(p-Methoxyphenyl)-3-phenyl-3-(2'-oxocyclohexyl)-1-propanone (73669-78-0) + trifluoroacetic acid (76-05-1) → 2-(4-Methoxyphenyl)-4-phenylcyclohexathiopyrylium Trifluoroacetate (73669-89-3) + 3-(4-Methoxyphenyl)-5-phenyl-2-thiabicyclo<4.4.0>decane (73669-96-2)

Guidance literature:

With hydrogen sulfide; Yield given; 1.) room temperature, overnight; 2.) reflux;

upstream raw materials:

1-(p-Methoxyphenyl)-3-phenyl-3-(2'-oxocyclohexyl)-1-propanone

2-(4-Methoxyphenyl)-4-phenyl-4H-cyclohexathiopyran

trifluoroacetic acid

Downstream raw materials:

(2S,4R)-2-(4-Methoxy-phenyl)-4-phenyl-3,4,5,6,7,8-hexahydro-2H-thiochromene

2α-(4-Methoxyphenyl)-4α-phenyl-cis-1-thiadecalin

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