Glycine, N-(cyclopropylcarbonyl)- (9CI)

Base Information

• Chemical Name: Glycine, N-(cyclopropylcarbonyl)- (9CI)
• CAS No.: 64513-70-8
• Molecular Formula: C6H9 N O3
• Molecular Weight: 143.14056
• Hs Code.: 2924299090
• Mol file: 64513-70-8.mol

Synonyms:Cyclopropylcarbonylglycine;N-Cyclopropylcarbonylglycine

Chemical Property of Glycine, N-(cyclopropylcarbonyl)- (9CI)

Chemical Property:

• Vapor Pressure: 9.22E-09mmHg at 25°C
• Boiling Point: 434.4°C at 760 mmHg
• Flash Point: 216.5°C
• PSA: 66.40000
• Density: 1.37g/cm³
• LogP: -0.01190

Purity/Quality:

99% ^*data from raw suppliers

2-(cyclopropylformamido)aceticacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Glycine, N-(cyclopropylcarbonyl)- (9CI)

There total 3 articles about Glycine, N-(cyclopropylcarbonyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.4%

cyclopropanecarboxylic acid chloride (4023-34-1) + glycine (56-40-6,18875-39-3,25718-94-9) → 2-(cyclopropanecarboxamido)acetic acid (64513-70-8)

Guidance literature:

With sodium carbonate; sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 4h;

Reference yield: 70.0%

ethyl 2-(cyclopropanecarboxamido)acetate (15924-92-2) → 2-(cyclopropanecarboxamido)acetic acid (64513-70-8)

Guidance literature:

With sodium hydroxide;

Reference yield:

→ 2-(cyclopropanecarboxamido)acetic acid (64513-70-8)

Guidance literature:

Cyclopropancarbonsaeure, 1.) SOCl2/Δ, 2.) Glycin/wss.NaOH/Dioxan;

upstream raw materials:

ethyl 2-(cyclopropanecarboxamido)acetate

cyclopropanecarboxylic acid chloride

glycine

Downstream raw materials:

C₂₀H₃₁N₂O₆P

Refernces

• 1、 -. "PYRONE COMPOUND AND ITS USE FOR PEST CONTROL". Page/Page column 282-283. . Retrieved 2011/05/06.