Technology Process of C26H36N2O5Si
There total 7 articles about C26H36N2O5Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C26H36N2O6Si;
With
triphenylphosphine; diethylazodicarboxylate;
In
toluene;
at 0 ℃;
for 1.5h;
With
2-nitrobenzenesulfonyl hydrazide;
In
tetrahydrofuran; water; toluene;
at 0 - 23 ℃;
for 23.1667h;
pH=7.0;
Aqueous potassium phosphate buffer solution;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium trifluoromethanesulfonate / toluene / 3 h / 23 - 60 °C / Inert atmosphere
1.2: 18 h / 23 °C / Inert atmosphere
2.1: diethylazodicarboxylate; triphenylphosphine / toluene / 1.5 h / 0 °C / Inert atmosphere
2.2: 23 h / 0 - 23 °C / Inert atmosphere
With
lithium trifluoromethanesulfonate; triphenylphosphine; diethylazodicarboxylate;
In
toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 10.5 h / 23 °C / Inert atmosphere
2.1: methanol; hexane; benzene / 0.08 h / 23 °C / Inert atmosphere
2.2: 0.5 h
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
3.2: 1 h / -78 °C / Inert atmosphere
4.1: lithium trifluoromethanesulfonate / toluene / 3 h / 23 - 60 °C / Inert atmosphere
4.2: 18 h / 23 °C / Inert atmosphere
5.1: diethylazodicarboxylate; triphenylphosphine / toluene / 1.5 h / 0 °C / Inert atmosphere
5.2: 23 h / 0 - 23 °C / Inert atmosphere
With
n-butyllithium; lithium trifluoromethanesulfonate; 3-chloro-benzenecarboperoxoic acid; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; hexane; ethyl acetate; toluene; benzene;