6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

Base Information

Chemical Name:6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide
CAS No.:133329-68-7
Molecular Formula:C₁₄H₁₅N₅O*HI
Molecular Weight:397.218
Hs Code.:

Synonyms:6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

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Technology Process of 6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

There total 3 articles about 6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 133329-67-6
7,9-dihydro-9-methyl-6-<(phenylmethyl)amino>-8H-purin-8-one

: 74-88-4
methyl iodide

: 133329-69-8
1,6,7,9-tetrahydro-1,9-dimethyl-6-<(phenylmethyl)imino>-8H-purin-8-one hydriodide

: 133329-68-7
6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

Guidance literature:: In N,N-dimethyl acetamide; at 46 ℃; for 79h;
DOI:10.1016/S0040-4039(00)71228-7

Reference yield:

: 133329-66-5
1-Benzyl-6-imino-9-methyl-1,6,7,9-tetrahydro-purin-8-one

: 133329-68-7
6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / 1N aq. NaOH / 1 h / Heating

2: 83 percent / N,N-dimethyl-acetamide / 79 h / 46 °C

With sodium hydroxide; In N,N-dimethyl acetamide;
DOI:10.1016/S0040-4039(00)71228-7

Reference yield:

: 119138-92-0
6-Amino-9-methyl-7H-purin-8(9H)-one

: 133329-68-7
6-[(Z)-Benzylimino]-3,9-dimethyl-3,6,7,9-tetrahydro-purin-8-one; hydriodide

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / N,N-dimethyl-acetamide / 6 h / 100 - 102 °C

2: 99 percent / 1N aq. NaOH / 1 h / Heating

3: 83 percent / N,N-dimethyl-acetamide / 79 h / 46 °C

With sodium hydroxide; In N,N-dimethyl acetamide;
DOI:10.1016/S0040-4039(00)71228-7