C₅₂H₅₄BF₂N₃S₂

Base Information

Chemical Name:C₅₂H₅₄BF₂N₃S₂
CAS No.:1533402-19-5
Molecular Formula:C₅₂H₅₄BF₂N₃S₂
Molecular Weight:833.961
Hs Code.:

C<sub>52</sub>H<sub>54</sub>BF<sub>2</sub>N<sub>3</sub>S<sub>2</sub>

Synonyms:C₅₂H₅₄BF₂N₃S₂

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Chemical Property of C₅₂H₅₄BF₂N₃S₂

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Technology Process of C₅₂H₅₄BF₂N₃S₂

There total 6 articles about C₅₂H₅₄BF₂N₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-63-7
boron trifluoride diethyl etherate

: C₅₂H₅₅N₃S₂

: 1533402-19-5
C₅₂H₅₄BF₂N₃S₂

Guidance literature:: With triethylamine; In toluene; at 80 ℃; for 0.5h;
DOI:10.1021/ol4034622

Reference yield:

: 92876-38-5
ethyl 2,6-dibromo-4H-thieno[3,2-b]pyrrole-5-carboxylate

: 1533402-19-5
C₅₂H₅₄BF₂N₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 12 h / Inert atmosphere; Schlenk technique; Heating

2: potassium hydroxide / ethylene glycol / 2 h / 130 °C / Inert atmosphere

3: acetic acid; acetic anhydride; sodium nitrite / 1.25 h / 0 - 80 °C

4: triethylamine / toluene / 0.5 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; acetic anhydride; sodium carbonate; acetic acid; triethylamine; potassium hydroxide; sodium nitrite; In ethylene glycol; toluene; 1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol4034622

Reference yield:

: 46193-76-4
ethyl 4H-thieno[3,2-b]pyrrole-5-carboxylate

: 1533402-19-5
C₅₂H₅₄BF₂N₃S₂

Guidance literature:: Multi-step reaction with 5 steps

1: bromine / dichloromethane / 1 h

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / toluene / 12 h / Inert atmosphere; Schlenk technique; Heating

3: potassium hydroxide / ethylene glycol / 2 h / 130 °C / Inert atmosphere

4: acetic acid; acetic anhydride; sodium nitrite / 1.25 h / 0 - 80 °C

5: triethylamine / toluene / 0.5 h / 80 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; acetic anhydride; sodium carbonate; acetic acid; triethylamine; potassium hydroxide; sodium nitrite; In dichloromethane; ethylene glycol; toluene; 2: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol4034622