Technology Process of C26H26F6O
There total 4 articles about C26H26F6O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 15 h / 70 °C / Inert atmosphere
2: hydrogenchloride / dichloromethane; ethanol; water / 5 h / 50 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); potassium carbonate;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2012.11.109
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrazine hydrate; sodium hydroxide
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 1 h / 0 °C
2.2: 24 h / 0 - 20 °C
3.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / tetrahydrofuran; hexane / 3 h / 0 °C / Inert atmosphere
3.2: 24 h / -78 °C / Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 15 h / 70 °C / Inert atmosphere
5.1: hydrogenchloride / dichloromethane; ethanol; water / 5 h / 50 °C
With
hydrogenchloride; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; N,N,N,N,-tetramethylethylenediamine; sodium hydride; potassium carbonate; hydrazine hydrate; sodium hydroxide;
In
tetrahydrofuran; ethanol; hexane; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.tetlet.2012.11.109
