3-Phenylacrylaldehyde N-phenylthiosemicarbazone

Base Information

Chemical Name:3-Phenylacrylaldehyde N-phenylthiosemicarbazone
CAS No.:72488-61-0
Molecular Formula:C₁₆H₁₅N₃S
Molecular Weight:281.381
Hs Code.:
European Community (EC) Number:655-930-5

Synonyms:AKOS003541304;Cinnamaldehyde, 4-phenyl-3-thiosemicarbazone;3-PHENYLACRYLALDEHYDE N-PHENYLTHIOSEMICARBAZONE;1-phenyl-3-[(E)-[(E)-3-phenylprop-2-enylidene]amino]thiourea

Suppliers and Price of 3-Phenylacrylaldehyde N-phenylthiosemicarbazone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Phenylacrylaldehyde N-phenylthiosemicarbazone

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:281.09866866
Heavy Atom Count:20
Complexity:340

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C=CC=NNC(=S)NC2=CC=CC=C2
Isomeric SMILES:C1=CC=C(C=C1)/C=C/C=N/NC(=S)NC2=CC=CC=C2

Technology Process of 3-Phenylacrylaldehyde N-phenylthiosemicarbazone

There total 6 articles about 3-Phenylacrylaldehyde N-phenylthiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 104-55-2
3-phenyl-propenal

: 5351-69-9
4-Phenyl-3-thiosemicarbazide

: 72488-61-0
3-phenyl-propenal 4-phenyl-thiosemicarbazone

Guidance literature:: With ethanol;

Reference yield:

: 51034-34-5
potassium aniline dithiocarbamate

: 72488-61-0
3-phenyl-propenal 4-phenyl-thiosemicarbazone

Guidance literature:: Multi-step reaction with 3 steps

1: H₂O / 24 h / 20 - 40 °C

2: hydrazine hydrate / methanol; H₂O / Heating

3: methanol / 3 h / Heating

With hydrazine hydrate; In methanol; water;
DOI:10.1016/j.saa.2004.11.035

Reference yield:

: 62-53-3
aniline

: 72488-61-0
3-phenyl-propenal 4-phenyl-thiosemicarbazone

Guidance literature:: Multi-step reaction with 4 steps

1: KOH / methanol; H₂O / 0 - 10 °C

2: H₂O / 24 h / 20 - 40 °C

3: hydrazine hydrate / methanol; H₂O / Heating

4: methanol / 3 h / Heating

With potassium hydroxide; hydrazine hydrate; In methanol; water;
DOI:10.1016/j.saa.2004.11.035