phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

Base Information

Chemical Name:phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate
CAS No.:813415-04-2
Molecular Formula:C₁₅H₁₉NO₃
Molecular Weight:261.321
Hs Code.:

Synonyms:phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

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Chemical Property of phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

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Technology Process of phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

There total 3 articles about phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 86507-74-6
3-(benzyloxy)-2,2-dimethyl-3-oxopropanoic acid

: 107-11-9,30551-89-4
1-amino-2-propene

: 813415-04-2
phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

Guidance literature:: With 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); triethylamine; In acetonitrile; at 20 ℃; for 0.333333h;
DOI:10.1002/ejoc.200400242

Reference yield:

: 57772-82-4
dibenzyl dimethylmalonate

: 813415-04-2
phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / KOH / phenylmethanol / 72 h

2: 92 percent / HCTU; triethylamine / acetonitrile / 0.33 h / 20 °C

With potassium hydroxide; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); triethylamine; In acetonitrile; benzyl alcohol;
DOI:10.1002/ejoc.200400242

Reference yield:

: 595-46-0
2,2-dimethylmalonic acid

: 813415-04-2
phenylmethyl 2-methyl-2-(2-propenyl)amidopropanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / DIEA; DMAP / CH₂Cl₂ / 24 h / 20 °C

2: 72 percent / KOH / phenylmethanol / 72 h

3: 92 percent / HCTU; triethylamine / acetonitrile / 0.33 h / 20 °C

With dmap; potassium hydroxide; 6-chloro-3-((dimethylamino)(dimethyliminio)methyl)-1H-benzo[d][1,2,3]triazol-3-ium-1-olatehexafluorophosphate(V); triethylamine; N-ethyl-N,N-diisopropylamine; In dichloromethane; acetonitrile; benzyl alcohol;
DOI:10.1002/ejoc.200400242