N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium

Base Information

• Chemical Name: N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium
• CAS No.: 134052-09-8
• Molecular Formula: C₆H₁₅N*C₃₅H₄₉N₅O₉
• Molecular Weight: 784.994

Synonyms:N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium

Chemical Property of N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium

Chemical Property:

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Technology Process of N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium

There total 6 articles about N¹-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine triethylammonium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

succinic acid anhydride (108-30-5) + N1-<<3-(3-aminobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-73-8) + triethylamine (121-44-8) → N1-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine triethylammonium (134052-09-8)

Guidance literature:

With dmap; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1016/0223-5234(91)90058-U

Reference yield:

N1,N5-di-boc-spermidine (68076-39-1) → N1-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine triethylammonium (134052-09-8)

Guidance literature:

Multi-step reaction with 5 steps

1: 55 percent / pyridine / acetonitrile / 3 h / Ambient temperature

2: 96 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

3: 92 percent / pyridine / acetonitrile / 1 h / Ambient temperature

4: 95 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

5: 85 percent / 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/0223-5234(91)90058-U

Reference yield:

N1-<(3-aminobenzen-1-yl)carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine (133765-71-6) → N1-<<3-<3-(succinamido)benzene-1-carboxamido>benzen-1-yl>carbonyl>-N4,N8-bis(tert-butoxycarbonyl)spermidine triethylammonium (134052-09-8)

Guidance literature:

Multi-step reaction with 3 steps

1: 92 percent / pyridine / acetonitrile / 1 h / Ambient temperature

2: 95 percent / H₂ / 10percent Pd/C / methanol / 4 h / 760 Torr / Ambient temperature

3: 85 percent / 4-dimethylaminopyridine (DMAP) / CH₂Cl₂ / 2 h / Ambient temperature

With pyridine; dmap; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;

DOI:10.1016/0223-5234(91)90058-U

upstream raw materials:

succinic acid anhydride

N¹-<<3-(3-aminobenzene-1-carboxamido)benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

triethylamine

N₁,N₅-di-boc-spermidine

Downstream raw materials:

N¹-<<3-<3-1-(spermidino)succinamido>benzene-1-carboxamido>benzen-1-yl>carbonyl>spermidine tetra(trifluoroacetate)

N¹-<<3-<3-4,N⁸-bis(tert-butoxycarbonyl)spermidinosuccinamido>benzene-1-carboxamido>benzen-1-yl>carbonyl>-N⁴,N⁸-bis(tert-butoxycarbonyl)spermidine

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