ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Base Information

Chemical Name:ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate
CAS No.:1446522-61-7
Molecular Formula:C₁₈H₂₁ClN₂O₇
Molecular Weight:412.827
Hs Code.:

Synonyms:ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

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Chemical Property of ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Chemical Property:

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Technology Process of ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

There total 3 articles about ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 582319-05-9
ethyl 7-chloroindole-3-(3-acetamido-3-carboethoxy)butanoate

: 1446522-61-7
ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Guidance literature:: With ozone; In methanol; for 1.5h; under 785.909 Torr; Cooling with acetone-dry ice;
DOI:10.1016/j.bmc.2013.05.039

Reference yield:

: 582320-17-0
ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

: 1446522-61-7
ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / water / 2 h / 55 - 60 °C

2: ozone / methanol / 1.5 h / 785.91 Torr / Cooling with acetone-dry ice

With sulfuric acid; ozone; In methanol; water;
DOI:10.1016/j.bmc.2013.05.039

Reference yield:

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 1446522-61-7
ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / benzene / 0.08 h

1.2: 20 °C / Cooling with ice

1.3: 60 h / 20 - 60 °C

2.1: sulfuric acid / water / 2 h / 55 - 60 °C

3.1: ozone / methanol / 1.5 h / 785.91 Torr / Cooling with acetone-dry ice

With sulfuric acid; sodium methylate; ozone; In methanol; water; benzene;
DOI:10.1016/j.bmc.2013.05.039