ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

Base Information

Chemical Name:ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone
CAS No.:582320-17-0
Molecular Formula:C₁₈H₂₄ClN₃O₅
Molecular Weight:397.859
Hs Code.:

Synonyms:ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

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Chemical Property of ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

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Technology Process of ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

There total 1 articles about ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 107-02-8,25068-14-8
acrolein

: 10449-07-7
(2-chlorophenyl)hydrazine

: 1068-90-2
2-acetylaminomalonic acid diethyl ester

: 582320-17-0
ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

Guidance literature:: 2-acetylaminomalonic acid diethyl ester; With sodium methylate; In benzene; for 0.0833333h;

acrolein; In benzene; at 20 ℃; Cooling with ice;

(2-chlorophenyl)hydrazine; With acetic acid; In benzene; at 20 - 60 ℃; for 60h;
DOI:10.1016/j.bmc.2013.05.039

Reference yield: 82.0%

: 582320-17-0
ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

: 582319-05-9
ethyl 7-chloroindole-3-(3-acetamido-3-carboethoxy)butanoate

Guidance literature:: With sulfuric acid; In water; at 55 - 60 ℃; for 2h;
DOI:10.1016/j.bmc.2013.05.039

Reference yield:

: 582320-17-0
ethyl 2-acetamido-2-carboethoxy-5-oxopentanoate 2-chlorophenylhydrazone

: 1446522-61-7
ethyl 2-acetamido-2-carboethoxy-5-oxo-5-(3-chloro-2-aminophenyl)pentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / water / 2 h / 55 - 60 °C

2: ozone / methanol / 1.5 h / 785.91 Torr / Cooling with acetone-dry ice

With sulfuric acid; ozone; In methanol; water;
DOI:10.1016/j.bmc.2013.05.039