4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside
CAS No.:866635-76-9
Molecular Formula:C₆₄H₇₃NO₁₃Si
Molecular Weight:1092.37
Hs Code.:

4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Synonyms:4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Chemical Property of 4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

There total 6 articles about 4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 866635-75-8
4-methoxyphenyl O-(3-O-allyl-2-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 100-39-0
benzyl bromide

: 866635-76-9
4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In tetrahydrofuran; at 0 ℃; for 3h;

Reference yield:

: 129575-89-9
p-methoxyphenyl 3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 866635-76-9
4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72.8 percent / Tf₂O; 2,6-di-tert-butylpyridine; molecular sieves 4 Angstroem / 1-benzenesulfinyl piperidine / CH₂Cl₂ / -60 - 0 °C

2: 95.6 percent / acetic acid / H₂O / 4 h / 60 °C

3: 84 percent / DMAP; imidazole / dimethylformamide / 3 h / 0 °C

4: 86 percent / NaH; Bu₄NI / tetrahydrofuran / 3 h / 0 °C

With 1H-imidazole; dmap; 2,6-di-tert-butyl-pyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; 1-benzenesulfinyl piperidine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 196697-67-3
(2R,4aR,6R,7S,8S,8aR)-8-Allyloxy-7-benzyloxy-2-phenyl-6-phenylsulfanyl-hexahydro-pyrano[3,2-d][1,3]dioxine

: 866635-76-9
4-methoxyphenyl O-(3-O-allyl-2,4-di-O-benzyl-6-O-tert-butyldimethylsilyl-β-D-mannopyranosyl)-(1->4)-3,6-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: 72.8 percent / Tf₂O; 2,6-di-tert-butylpyridine; molecular sieves 4 Angstroem / 1-benzenesulfinyl piperidine / CH₂Cl₂ / -60 - 0 °C

2: 95.6 percent / acetic acid / H₂O / 4 h / 60 °C

3: 84 percent / DMAP; imidazole / dimethylformamide / 3 h / 0 °C

4: 86 percent / NaH; Bu₄NI / tetrahydrofuran / 3 h / 0 °C

With 1H-imidazole; dmap; 2,6-di-tert-butyl-pyridine; trifluoromethylsulfonic anhydride; 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; sodium hydride; acetic acid; 1-benzenesulfinyl piperidine; In tetrahydrofuran; dichloromethane; water; N,N-dimethyl-formamide;