C₃₀H₄₀BrN₃O₉S

Base Information

Chemical Name:C₃₀H₄₀BrN₃O₉S
CAS No.:861397-55-9
Molecular Formula:C₃₀H₄₀BrN₃O₉S
Molecular Weight:698.632
Hs Code.:

C<sub>30</sub>H<sub>40</sub>BrN<sub>3</sub>O<sub>9</sub>S

Synonyms:C₃₀H₄₀BrN₃O₉S

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Chemical Property of C₃₀H₄₀BrN₃O₉S

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Technology Process of C₃₀H₄₀BrN₃O₉S

There total 6 articles about C₃₀H₄₀BrN₃O₉S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1309888-72-9
C₃₂H₄₄BrN₃O₉S

: 861397-55-9
C₃₀H₄₀BrN₃O₉S

Guidance literature:: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris(hydroxymethyl)phosphine; In toluene; at 50 - 80 ℃; for 2.5h; Inert atmosphere;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 861397-55-9
C₃₀H₄₀BrN₃O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 20 °C

1.2: pH ~ 3 / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.33 h / 20 °C

2.2: 16 h

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris(hydroxymethyl)phosphine / toluene / 2.5 h / 50 - 80 °C / Inert atmosphere

With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris(hydroxymethyl)phosphine; In 1,4-dioxane; dichloromethane; water; toluene;

Reference yield:

: 801282-60-0
C₂₃H₂₉BrN₂O₈S

: 861397-55-9
C₃₀H₄₀BrN₃O₉S

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride / ethyl acetate; 1,4-dioxane / 3.5 h / 20 - 25 °C

2.1: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / dichloromethane / 0.33 h / 20 °C

2.2: 16 h

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris(hydroxymethyl)phosphine / toluene / 2.5 h / 50 - 80 °C / Inert atmosphere

With hydrogenchloride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; tris(hydroxymethyl)phosphine; In 1,4-dioxane; dichloromethane; ethyl acetate; toluene;