4-CHLORO-N-(4-CHLOROPHENYL)BENZAMIDE

Base Information

• Chemical Name: 4-CHLORO-N-(4-CHLOROPHENYL)BENZAMIDE
• CAS No.: 39193-06-1
• Molecular Formula: C13H9Cl2NO
• Molecular Weight: 266.127
• Mol file: 39193-06-1.mol

Synonyms:4-Chlor-benzoesaeure-(4-chlor-anilid);4,4'-Dichlorobenzanilide;n1-(4-chlorophenyl)-4-chlorobenzamide;N-(p-chlorophenyl)-p-chlorobenzamide;Benzamide,4-chloro-N-(4-chlorophenyl);4-chloro-N-(4-chlorophenyl)-benzamid;4-chloro-benzoic acid-(4-chloro-anilide);N-(p-Chlorobenzoyl)-p-chloraniline;

Chemical Property of 4-CHLORO-N-(4-CHLOROPHENYL)BENZAMIDE

Chemical Property:

• Vapor Pressure: 0.000408mmHg at 25°C
• Boiling Point: 316.5°Cat760mmHg
• Flash Point: 145.2°C
• PSA: 29.10000
• Density: 1.384g/cm³
• LogP: 4.31870

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-CHLORO-N-(4-CHLOROPHENYL)BENZAMIDE

There total 31 articles about 4-CHLORO-N-(4-CHLOROPHENYL)BENZAMIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

C16H13Cl2NO3 → 4,4'-dichlorobenzanilide (39193-06-1)

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 25 ℃; for 12h;

DOI:10.1016/S0040-4039(00)00875-3

Reference yield: 98.0%

C14H10Cl2N2O2 → 4,4'-dichlorobenzanilide (39193-06-1)

Guidance literature:

With sulfuric acid; isopentyl nitrite; at 0 - 25 ℃; for 6.5h;

DOI:10.1016/S0040-4039(00)01243-0

Reference yield: 97.0%

4,4'-dichlorobenzophenone oxime (1714-50-7) → 4,4'-dichlorobenzanilide (39193-06-1)

Guidance literature:

With FeCl₃-montmorillonite; In toluene; for 0.133333h; Heating;

DOI:10.1080/00397919708006036

upstream raw materials:

4,4'-dichlorobenzophenone oxime

ethylmagnesium bromide

4-chloro-aniline

4-chloro-benzoyl chloride

Downstream raw materials:

4-chloro-N-(4-chlorobenzyl)aniline

6-chloro-2-(4-chlorophenyl)benzo[d]oxazole

4-chloro-aniline

N-(4-Chloro-phenyl)-N'-(4-nitro-phenyl)-formamidine

Refernces

• 1、 Bhattacherjee, Dhananjay,Das, Pralay,Giri, Kousik,Shaifali,Sharma, Ajay Kumar,Sharma, Navneet,Sheetal. "Supported-Pd catalyzed tandem approach for N-arylbenzamides synthesis". . . Retrieved 2021/11/24.
• 2、 Lockley, William J.S.,Venanzi, Niccolò A. E.,Crane, Georgie J.. "Studies of hydrogen isotope scrambling during the dehalogenation of aromatic chloro-compounds with deuterium gas over palladium catalysts". . p. 531 - 552. Retrieved 2020/09/22.