2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Base Information

• Chemical Name: 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine
• CAS No.: 101515-75-7
• Molecular Formula: C₂₃H₁₈N₂O₂S₂
• Molecular Weight: 418.54

Synonyms:2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Chemical Property of 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

Chemical Property:

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Technology Process of 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine

There total 2 articles about 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.5%

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt (101515-73-5) + benzoyl chloride (98-88-4) → 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (101515-75-7)

Guidance literature:

In benzene; for 6h; Ambient temperature;

DOI:10.1007/BF00515244

Reference yield: 38.8%

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt (101515-73-5) + benzoyl chloride (98-88-4) → 2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (101515-75-7) + 1-benzoyl-2-thio-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (101515-77-9)

Guidance literature:

In neat (no solvent); at 100 ℃; for 2.7h;

DOI:10.1007/BF00515244

Reference yield:

2-mercaptobenzoyl-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine (101515-75-7) → Benzoyl bromide (618-32-6) + bis(3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidin-2-yl) disulfide (101515-79-1)

Guidance literature:

With bromine; In tetrachloromethane; Yield given; Ambient temperature;

DOI:10.1007/BF00515244

upstream raw materials:

2-mercapto-3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidine sodium salt

benzoyl chloride

Downstream raw materials:

Benzoyl bromide

bis(3-phenyl-4-oxo-3,4,5,6,7,8-hexahydrobenzothieno<2,3-d>pyrimidin-2-yl) disulfide

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