trans-2,trans-3-diphenylcyclopropanecarboxaldehyde

Base Information

Chemical Name:trans-2,trans-3-diphenylcyclopropanecarboxaldehyde
CAS No.:64200-26-6
Molecular Formula:C₁₆H₁₄O
Molecular Weight:222.287
Hs Code.:

Synonyms:trans-2,trans-3-diphenylcyclopropanecarboxaldehyde

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Chemical Property of trans-2,trans-3-diphenylcyclopropanecarboxaldehyde

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Technology Process of trans-2,trans-3-diphenylcyclopropanecarboxaldehyde

There total 16 articles about trans-2,trans-3-diphenylcyclopropanecarboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7381-90-0,7381-98-8,26848-96-4
cis, trans-1-hydroxymethyl-2,3-diphenylcyclopropane

: 52456-99-2,64200-26-6,102519-32-4
trans-2,3-diphenylcyclopropane-1-carbaldehyde

Guidance literature:: cis, trans-1-hydroxymethyl-2,3-diphenylcyclopropane; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 1h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1039/c9ob00359b

Reference yield: 94.0%

: 7381-98-8
trans, trans-1-hydroxymethyl-2,3-diphenylcyclopropane

: 64200-26-6
trans-2,trans-3-diphenylcyclopropanecarboxaldehyde

Guidance literature:: With 1-methyl-1H-imidazole; [2,2]bipyridinyl; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate; oxygen; In acetonitrile; at 20 ℃;
DOI:10.1021/ja5070137

Reference yield: 71.0%

: 61608-79-5
((1R*,2R*)-3-bromocyclopropane-1,2-diyl)dibenzene

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 52456-99-2,64200-26-6,102519-32-4
trans-2,3-diphenylcyclopropane-1-carbaldehyde

Guidance literature:: ((1R*,2R*)-3-bromocyclopropane-1,2-diyl)dibenzene; With TurboGrignard; In tetrahydrofuran; 1,4-dioxane; at -16 ℃; for 14h;

N,N-dimethyl-formamide; In tetrahydrofuran; 1,4-dioxane; stereoselective reaction;
DOI:10.1055/s-0028-1087487