tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester

Base Information

• Chemical Name: tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester
• CAS No.: 100813-26-1
• Molecular Formula: C₇H₁₀O₄
• Molecular Weight: 158.154
• Mol file: 100813-26-1.mol

Synonyms:tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester

Chemical Property of tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester

Chemical Property:

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Technology Process of tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester

There total 1 articles about tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

2-hydroxy-3-methylcyclopent-2-en-1-one (80-71-7) → tetrahydro-2-methyl-5-oxo-2-furancarboxylic acid methyl ester (100813-26-1) + methyl 4-carboxy-2-hydroxy-2-methylbutanoate (100813-24-9) + levulinic acid (123-76-2)

Guidance literature:

With oxygen; rose bengal; In methanol; at 40 ℃; for 13h; Title compound not separated from byproducts; Irradiation;

DOI:10.1021/jo00357a042

upstream raw materials:

2-hydroxy-3-methylcyclopent-2-en-1-one