N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

Base Information

Chemical Name:N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide
CAS No.:1062174-70-2
Molecular Formula:C₄₁H₃₈N₂O₆
Molecular Weight:654.763
Hs Code.:

Synonyms:N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

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Chemical Property of N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

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Technology Process of N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

There total 3 articles about N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40615-36-9
4,4'-dimethoxytrityl chloride

: N,N'-bis(2-hydroxyethyl)phenathrene-3,6-dicarboxamide

: 1062174-70-2
N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

Guidance literature:: With pyridine; at 20 ℃; for 2h;
DOI:10.1002/hlca.200390256

Reference yield:

: 141-43-5
ethanolamine

: 153765-10-7
2-(bis(4-methoxyphenyl)(phenyl)methoxy)ethanamine

: 59795-45-8
phenanthrene-3,6-dicarboxylic acid

: 1062174-70-2
N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;
DOI:10.1080/15257770701506319

Reference yield:

: 181509-97-7
dimethyl phenanthrene-3,6-dicarboxylate

: 1062174-70-2
N-{2-[(4,4'-dimethoxytrityl)oxy]ethyl}-N'-(2-hydroxyethyl)phenanthrene-3,6-dicarboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 0.5 h / 175 °C

2: 1.391 g / pyridine / 2 h / 20 °C

With pyridine;
DOI:10.1002/hlca.200390256