6-bromo-2,3-dimethoxybenzyl cyanide

Base Information

Chemical Name:6-bromo-2,3-dimethoxybenzyl cyanide
CAS No.:107290-29-9
Molecular Formula:C₁₀H₁₀BrNO₂
Molecular Weight:256.099
Hs Code.:

Synonyms:6-bromo-2,3-dimethoxybenzyl cyanide

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Chemical Property of 6-bromo-2,3-dimethoxybenzyl cyanide

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Technology Process of 6-bromo-2,3-dimethoxybenzyl cyanide

There total 3 articles about 6-bromo-2,3-dimethoxybenzyl cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.8%

: 143-33-9,25596-52-5
sodium cyanide

: 107290-28-8
6-bromo-2,3-dimethoxybenzyl chloride

: 107290-29-9
6-bromo-2,3-dimethoxybenzyl cyanide

Guidance literature:: In dimethyl sulfoxide; at 40 - 50 ℃; for 1h;

Reference yield:

: 53811-50-0
6-bromo-2,3-dimethoxybenzaldehyde

: 107290-29-9
6-bromo-2,3-dimethoxybenzyl cyanide

Guidance literature:: Multi-step reaction with 3 steps

1: 83.8 percent / NaBH₄ / tetrahydrofuran / 1 h / Ambient temperature

2: 94.1 percent / thionyl chloride, N,N-dimethylaniline / benzene / 1 h, room temperature, 30 min, 100 degC

3: 91.8 percent / dimethylsulfoxide / 1 h / 40 - 50 °C

With sodium tetrahydroborate; thionyl chloride; N,N-dimethyl-aniline; In tetrahydrofuran; dimethyl sulfoxide; benzene;

Reference yield:

: 107290-27-7
(6-bromo-2,3-dimethoxyphenyl)methanol

: 107290-29-9
6-bromo-2,3-dimethoxybenzyl cyanide

Guidance literature:: Multi-step reaction with 2 steps

1: 94.1 percent / thionyl chloride, N,N-dimethylaniline / benzene / 1 h, room temperature, 30 min, 100 degC

2: 91.8 percent / dimethylsulfoxide / 1 h / 40 - 50 °C

With thionyl chloride; N,N-dimethyl-aniline; In dimethyl sulfoxide; benzene;