Technology Process of C57H100N2O14S
There total 6 articles about C57H100N2O14S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% palladium on activated charcoal; ammonium formate;
In
tetrahydrofuran; methanol;
at 60 ℃;
for 0.5h;
DOI:10.1016/j.bmcl.2011.03.056
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 36 h / 24 °C
2: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 8 h / 90 °C
3: cadmium(II) carbonate / benzene / 1.5 h / Reflux
4: 10% palladium on activated charcoal; ammonium formate / tetrahydrofuran; methanol / 0.5 h / 60 °C
With
cadmium(II) carbonate; 10% palladium on activated charcoal; ammonium formate; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.bmcl.2011.03.056
- Guidance literature:
-
Multi-step reaction with 4 steps
1: triethylamine / dichloromethane / 36 h / 24 °C
2: tetra-(n-butyl)ammonium iodide; caesium carbonate / N,N-dimethyl-formamide / 8 h / 90 °C
3: cadmium(II) carbonate / benzene / 1.5 h / Reflux
4: 10% palladium on activated charcoal; ammonium formate / tetrahydrofuran; methanol / 0.5 h / 60 °C
With
cadmium(II) carbonate; 10% palladium on activated charcoal; ammonium formate; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; benzene;
DOI:10.1016/j.bmcl.2011.03.056
