tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

Base Information

Chemical Name:tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate
CAS No.:1439361-95-1
Molecular Formula:C₂₅H₂₉N₃O₆S
Molecular Weight:499.588
Hs Code.:

Synonyms:tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

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Chemical Property of tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

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Technology Process of tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

There total 4 articles about tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1022542-98-8
C₁₇H₁₄N₂O₄S

: 83948-53-2
3-bromopropylamine tert-butylcarbamate

: 1439361-95-1
tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 4h;
DOI:10.1002/cmdc.201200390

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1439361-95-1
tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / methanol; acetonitrile

2: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

With potassium carbonate; triethylamine; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201200390

Reference yield:

: 86-53-3
1-Cyanonaphthalene

: 1439361-95-1
tert-butyl 3-(N-(naphthalen-1-ylmethyl)-2-nitrophenylsulfonamido)propylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C

2: triethylamine / tetrahydrofuran

3: potassium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C

With lithium aluminium tetrahydride; potassium carbonate; triethylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201200390