2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol

Base Information

• Chemical Name: 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol
• CAS No.: 1584677-20-2
• Molecular Formula: C₁₈H₃₀O₅S₂
• Molecular Weight: 390.565

Synonyms:2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol

Chemical Property of 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol

Chemical Property:

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Technology Process of 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol

There total 2 articles about 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-(allyloxy)-1-((allyloxy)methyl)-3-methoxy benzene (1064703-83-8) + 2-hydroxyethanethiol (60-24-2) → 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol (1584677-20-2)

Guidance literature:

In neat (no solvent); UV-irradiation;

DOI:10.1039/c3gc42613k

Reference yield:

4-hydroxymethyl-2-methoxyphenol (498-00-0) → 2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol (1584677-20-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water / 0.17 h / 50 °C

1.2: 5 h

2.1: neat (no solvent) / UV-irradiation

With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water;

DOI:10.1039/c3gc42613k

Reference yield: 88.0%

2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol (1584677-20-2) → 2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine (1584677-23-5)

Guidance literature:

With 2-mercaptoethylamine hydrochloride; In methanol; UV-irradiation;

DOI:10.1039/c3gc42613k

upstream raw materials:

4-(allyloxy)-1-((allyloxy)methyl)-3-methoxy benzene

2-hydroxyethanethiol

4-hydroxymethyl-2-methoxyphenol

Downstream raw materials:

2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

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