2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

Base Information

Chemical Name:2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine
CAS No.:1584677-23-5
Molecular Formula:C₁₈H₃₂N₂O₃S₂
Molecular Weight:388.596
Hs Code.:

Synonyms:2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

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Chemical Property of 2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

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Technology Process of 2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

There total 3 articles about 2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1584677-20-2
2-((3-((4-(3-((2-hydroxyethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-ol

: 1584677-23-5
2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

Guidance literature:: With 2-mercaptoethylamine hydrochloride; In methanol; UV-irradiation;
DOI:10.1039/c3gc42613k

Reference yield:

: 1064703-83-8
4-(allyloxy)-1-((allyloxy)methyl)-3-methoxy benzene

: 1584677-23-5
2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: neat (no solvent) / UV-irradiation

2: 2-mercaptoethylamine hydrochloride / methanol / UV-irradiation

With 2-mercaptoethylamine hydrochloride; In methanol;
DOI:10.1039/c3gc42613k

Reference yield:

: 498-00-0
4-hydroxymethyl-2-methoxyphenol

: 1584677-23-5
2-((3-((4-(3-((2-aminoethyl)thio)propoxy)-3-methoxybenzyl)oxy)propyl)thio)ethan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide / water / 0.17 h / 50 °C

1.2: 5 h

2.1: neat (no solvent) / UV-irradiation

3.1: 2-mercaptoethylamine hydrochloride / methanol / UV-irradiation

With N-benzyl-N,N,N-triethylammonium chloride; 2-mercaptoethylamine hydrochloride; sodium hydroxide; In methanol; water;
DOI:10.1039/c3gc42613k